Nanowires made of ternary alloys – synthesis features and magnetic properties

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Nanowires of FexCoyCu(100–x–y) and FexNiyCu(100–x–y) alloys have been studied. The features of obtaining such structures by the matrix synthesis method have been investigated. Elemental analysis of nanowires grown at sequentially increasing voltages revealed a significant decrease in the amount of copper, as well as a change in the ratio of the main magnetic elements. X-ray phase analysis showed that FeCoCu is a three-component solid solution, while FeNiCu contains three phases of solid solutions: FeCu with copper content up to 80%, FeNi with high iron content, and NiCu in an amorphous or fine-crystalline state with nickel content up to 80%. Mössbauer spectroscopy revealed that the addition of copper can lead to a change in the angle of magnetic moment misalignment in nanowires, which correlates with magnetometry data.

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作者简介

D. Khairetdinova

National University of Science and Technology “MISIS”; Shubnikov Institute of Crystallography of Kurchatov Complex of Crystallography and Photonics of NRC “Kurchatov Institute”

编辑信件的主要联系方式.
Email: hairetdr@gmail.com

Smart Sensors Laboratory, Department of Electronic Materials Technology

俄罗斯联邦, Moscow; Moscow

I. Doludenko

Shubnikov Institute of Crystallography of Kurchatov Complex of Crystallography and Photonics of NRC “Kurchatov Institute”

Email: hairetdr@gmail.com
俄罗斯联邦, Moscow

I. Perunov

Shubnikov Institute of Crystallography of Kurchatov Complex of Crystallography and Photonics of NRC “Kurchatov Institute”

Email: hairetdr@gmail.com
俄罗斯联邦, Moscow

I. Volchkov

Shubnikov Institute of Crystallography of Kurchatov Complex of Crystallography and Photonics of NRC “Kurchatov Institute”

Email: hairetdr@gmail.com
俄罗斯联邦, Moscow

L. Panina

National University of Science and Technology “MISIS”

Email: hairetdr@gmail.com
俄罗斯联邦, Moscow

D. Zagorskiy

Shubnikov Institute of Crystallography of Kurchatov Complex of Crystallography and Photonics of NRC “Kurchatov Institute”

Email: hairetdr@gmail.com
俄罗斯联邦, Moscow

K. Frolov

Shubnikov Institute of Crystallography of Kurchatov Complex of Crystallography and Photonics of NRC “Kurchatov Institute”

Email: hairetdr@gmail.com
俄罗斯联邦, Moscow

V. Kanevskii

Shubnikov Institute of Crystallography of Kurchatov Complex of Crystallography and Photonics of NRC “Kurchatov Institute”

Email: hairetdr@gmail.com
俄罗斯联邦, Moscow

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2. Fig. 1. Polarization curves for the compositions: a – FexCoyCu(100–x–y), b – FexNiyCu(100–x–y). Vertical dashed lines indicate the potentials of the onset of deposition of the corresponding metal.

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3. Fig. 2. Examples of SEM images of NP obtained at a deposition voltage of 1.8 V: a – Fe36Co59Cu5, b – Fe61Ni31Cu8.

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4. Fig. 3. Dependence of the NP composition on the deposition voltage: a – FexCoyCu(100–x–y), b – FexNiyCu(100–x–y). The compositions studied in detail in this work are highlighted.

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5. Fig. 4. X–ray diffractograms of NP samples: a – FexCoyCu(100–x-y), b – FexNiyCu(100–x–y). The insets show enlarged areas in the intervals 42-48 and additionally in the interval 48-55 for (b).

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6. Fig. 5. Mossbauer spectra of NP samples: a – Fe36Co59Cu5, b – Fe39Ni35Cu26. The dark color indicates the ferromagnetic component, the light color indicates the paramagnetic component.

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7. Fig. 6. Magnetic hysteresis loops for NP: a – Fe36Co59Cu5, b – Fe61Ni31Cu8.

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