Coordination Polymers Ca(II)–Cr(III) and Ba(II)–Cr(III) with Cyclobutane-1,1-dicarboxylic Acid Anions

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The reactions of Cr(NO3)3 ⋅ 9H2O with barium and calcium salts of cyclobutane-1,1-dicarboxylic acid (H2Cbdc) in a ratio of 1 : 3 in an aqueous solution are studied. The reaction products isolated in the crystalline state are shown to be compounds formed by the binuclear tetraanionic units Cr2(OH)2(Cbdc)4] 4−, and the nature of the alkaline-earth metal ion introduced into the synthesis affects the dimensionality of the formed polymeric structure. The 2D polymeric compound Ba2Cr2(OH)2(Cbdc)4(H2O)5] ⋅ 3H2O}𝑛 (I) is formed in the reaction with Ba(Cbdc), and the replacement of Ba2+ by Ca2+ results in the formation of the 1D coordination polymer { Ca2Cr2(OH)(Cbdc)4(H2O)6] ⋅ 8H2O}𝑛 (II). The crystal structures of compounds I and II are determined by single-crystal XRD (CIF files CCDC nos. 2344872 (I) and 2344873 (II), respectively).

作者简介

E. Bazhina

Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences

Email: evgenia-VO@mail.ru
Moscow, Russia

M. Shmelev

Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences

Moscow, Russia

M. Kiskin

Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences

Moscow, Russia

I. Eremenko

Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences

Moscow, Russia

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